激光剥蚀等离子体质谱分析中激光剥蚀参数对信号响应的影响   总被引：5，自引：1，他引：5  

徐鸿志靳兰兰  李爱荣帅琴 胡圣虹 《岩矿测试》2005,24(3):171-175

探讨了激光剥蚀等离子体质谱固体微区分析中激光剥蚀参数对元素分析信号灵敏度及稳定性的影响。这些参数包括激光功率、脉冲频率、剥蚀孔经、散焦距离、剥蚀方式等。讨论了优化的激光剥蚀等离子体质谱信号采集及数据处理方式。在全质量范围内选用具有代表性的元素作为研究对象,建立了激光剥蚀的一般性特征规律和266nm紫外激光系统的最佳操作条件。在选定的激光剥蚀参数下,大多数被测元素的检出限为22.8~457ng/g,能够满足固体微区分析的要求。  相似文献   

"嫦娥"卫星绕月飞行轨道的激光测定法     

刘基余 《武汉大学学报(信息科学版)》2005,30(10):870-872,880

依据地月激光测距的成功实践和对卫星激光定轨的基础研究,提出了用地面对嫦娥卫星作激光测距的方法,高精度地测定嫦娥卫星绕月飞行时的实时在轨位置,论述了多站激光定轨和单站激光定轨的解算数模。  相似文献   

Combined Digital Photogrammetry and Time-of-Flight Laser Scanning for Monitoring Cliff Evolution   总被引：4，自引：0，他引：4  

Michael  Lim  David N.  Petley  Nicholas J.  Rosser  Robert J.  Allison  Antony J.  Long  David  Pybus 《The Photogrammetric Record》2005,20(110):109-129

Although cliffs form approximately 75% of the world's coastline, the understanding of the processes through which they evolve remains limited because of a lack of quantitative data on the morphological changes they undergo. In this paper the combination of terrestrial time-of-flight laser scanning with high-resolution digital photogrammetry is examined to generate high-quality data-sets pertaining to the geomorphic processes governing cliff development. The study was undertaken on a section of hard rock cliffs in North Yorkshire, UK, which has been monitored over a 12-month period. High-density, laser-scanned point clouds have been used to produce an accurate representation of these complex surfaces, free from the optical variations that degrade photographic data. These data-sets have been combined with high-resolution photographic monitoring, resampled with the fixed accuracies of the terrestrial laser survey, to generate a new approach to recording the volumetric changes in complex coastal cliffs. This has led to significant improvements in the understanding of the activity patterns of coastal cliffs.  相似文献   

Spectral Filtering and Classification of Terrestrial Laser Scanner Point Clouds   总被引：1，自引：0，他引：1  

Derek D.  Lichti 《The Photogrammetric Record》2005,20(111):218-240

A method is presented for filtering and classification of terrestrial laser scanner point clouds. The algorithm exploits the four-channel (blue, green, red and near infrared) multispectral imaging capability of some terrestrial scanners using supervised, parametric classification to assign thematic class labels to all scan cloud points. Its principal advantage is that it is a completely data-driven algorithm and is independent of spatial sampling resolution since the processing is performed in four-dimensional spectral feature space. Its application to two data-sets of different spatial extent and spatial and spectral complexity is reported, for which respective overall classification accuracies of 87·0% and 82·0% were achieved. Analysis of the input data with emphasis on the characteristics pertinent to the anticipated outcomes precedes detailed analysis of the classification results and error sources and their causes. Erroneously classified points are attributed to radiometric errors stemming from both detector hardware and physical effects.  相似文献   

图像处理技术在地质灾害监测中的应用   总被引：1，自引：0，他引：1  

冯苍旭  史云  陈实 《中国地质灾害与防治学报》2003,14(2):84-86

三维激光微位移监测技术是一种对地质灾害进行长期监测的新方法。该技术用激光作为光源，用CCD摄像器作为镜头，通过图象采集卡把视频信号采入计算机中，用与该仪器配套的专门软件对采集到的光斑图像进行处理，计算出光斑的三维中心坐标值，把该值和原点坐标值进行比较，就可以算出灾害体滑动的距离。该系统可以对灾害体进行长期、非接触监测，监测时间、监测频率可以任意设定。文章概括介绍该监测的原理，各个组成部分，重点介绍软件部分，即采集的视频信号进入计算机后的图像处理过程和数据库结构。该监测系统已在三块地区试运行了3个月，效果较好。  相似文献   

机载激光测深中的波浪改正技术   总被引：3，自引：0，他引：3  

黄谟涛  翟国君  欧阳永忠  陆秀平 《武汉大学学报(信息科学版)》2003,28(4):389-392

基于我国新研制的机载激光测深系统基本配置，提出了3种可供选择的波浪改正计算方案(也称为深度值归算方案)，具体分析了3种方案的适用条件和应用范围，并从理论上对3种改正模型的计算精度进行了估算。  相似文献   

从激光扫描数据中进行建筑物特征提取研究   总被引：42，自引：4，他引：42  

李必军  方志祥  任娟 《武汉大学学报(信息科学版)》2003,28(1):65-70

提出了一套基于建筑物几何特征的信息挖掘方案，并具体介绍了研究中采用的一些原理、方法与实用算法，从而可以直接从激光扫描数据中提取建筑物的平面外轮廓信息。利用本方案对车载激光扫描系统获取的城市建筑物试验数据进行了具体的处理，并给出了三维建模和可视化表达结果。  相似文献   

Preliminary Results from a New 157 nm Laser Ablation ICP-MS Instrument: New Opportunities in the Analysis of Solid Samples     

Philippe Telouk  Estelle F. Rose-Koga  Francis Albarede 《Geostandards and Geoanalytical Research》2003,27(1):5-11

Preliminary results are given from an excimer 157 nm laser ablation multiple-collector inductively coupled plasma-mass spectrometer (LA-MC-ICP-MS), used for the isotopic measurements of solid materials. Elements of geological interest with different volatilities such as Pb and U (e.g. zircon geochronology) and Cu and Zn (as examples of geochemical/biochemical tracers) were analysed. The range of ablation rates of 20-150 nm s^-1 enabled us to ablate the sample down to a depth of 45 μm for a 50 μm diameter pit. The Cu and Zn isotopic measurements gave values that were very stable with, on average, a 0.01 % standard error, comparable with that achieved in liquid mode measurements.  相似文献   

Laser Ablation ICP-MS Analysis of Geological Materials Prepared as Lithium Borate Glasses   总被引：9，自引：0，他引：9  

Stephen M. Eggins 《Geostandards and Geoanalytical Research》2003,27(2):147-162

A simple, rapid and precise method is described for determining trace elements by laser ablation (LA)-ICP-MS analysis in bulk geological materials that have been prepared as lithium borate glasses following standard procedures for XRF analysis. This approach reliably achieves complete sample digestion and provides for complementary XRF and LA-ICP-MS analysis of a full suite of major and trace elements from a single sample preparation. Highly precise analysis is enabled by rastering an ArF excimer laser (λ= 193nm) across fused samples to deliver a constant sample yield to the mass spectrometer without inter-element fractionation effects during each analysis. Capabilities of the method are demonstrated by determination of twenty five trace elements (Sc, Ti, V, Ga, Rb, Sr, Y, Zr, Nb, Cs, Ba, REE, Hf, Ta, Pb, Th and U) in a diverse range of geological reference materials that includes peridotites, basalts, granites, metamorphic rocks and sediments. More than 90% of determinations are indistinguishable from published reference values at the 95% confidence level. Systematic bias greater than 5% is observed for only a handful of elements (Zr, Nb and U) and may be attributed in part to inaccurate calibration values used for the NIST SRM 612 glass in the case of Zr and Nb. Detection limits for several elements, most notably La, are compromised at ultra-trace levels by impurities in the lithium borate flux but can be corrected for by subtracting appropriate procedural blanks. Reliable Pb analysis has proved problematic due to variable degrees of contamination introduced during sample polishing prior to analysis and from Pt-crucibles previously used to fuse Pb-rich samples. Scope exists for extending the method to include internal standard element/isotope spiking, particularly where integrated XRF analysis is not available to characterise major and trace elements in the fused lithium borate glasses prior to LA-ICP-MS analysis.  相似文献   

A Reappraisal of Rb, Y, Zr, Pb and Th Values in Geochemical Reference Material BHVO-1     

William J. Chazey III  Clive R. Neal  Jinesh C. Jain  William S. Kinman 《Geostandards and Geoanalytical Research》2003,27(2):181-192

The geochemical reference material BHVO-1 was analysed by a variety of techniques over a six year period. These techniques included inductively coupled plasma-mass spectrometry and atomic emission spectroscopy (ICP-MS and ICP-AES, respectively), laser ablation ICP-MS and spark source mass spectroscopy. Inconsistencies between the published consensus values reported by Gladney and Roelandts (1988, Geostandards Newsletter) and the results of our study are noted for Rb, Y, Zr, Pb and Th. The values reported here for Rb, Y, Zr and Pb are generally lower, while Th is higher than the consensus value. This is not an analytical artefact unique to the University of Notre Dame ICP-MS facility, as most of the BHVO-1 analyses reported over the last ten to twenty years are in agreement with our results. We propose new consensus values for each of these elements as follows: Rb = 9.3 ± 0.2 μg g-1 (compared to 11 ± 2 μg g-1), Y = 24.4 ± 1.3 μg g-1 (compared to 27.6 ± 1.7 μg g-1), Zr = 172 ± 10 μg g-1 (compared to 179 ± 21 μg g-1), Pb = 2.2 ± 0.2 μg g-1 (compared to 2.6 ± 0.9 μg g-1) and Th = 1.22 ± 0.02 μg g-1 (compared to 1.08 ± 0.15 μg g-1).  相似文献